PUKYONG

study on the fabrication of graphene using the exfoliation method

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Abstract
The effect of various synthesis conditions in the fabrication of graphene using the exfoliation method has been investigated. The graphite oxide and graphene fabricated by various synthesis conditions were identified by SEM, FE-SEM and XRD. Graphite oxide was fabricated from graphite using chemical exfoliation and graphene was manufactured from graphite oxide by thermal exfoliation. As a result, graphite oxide was well formed from graphite and graphene could be obtained from graphite oxide. And it was found that the interlayer spacing between the graphene layers depended on the reaction time and particle size, regardless of the reaction temperature from 5℃ to 25℃.
Author(s)
이정수
Issued Date
2014
Awarded Date
2014. 2
Type
Dissertation
Publisher
부경대학교
URI
https://repository.pknu.ac.kr:8443/handle/2021.oak/1422
http://pknu.dcollection.net/jsp/common/DcLoOrgPer.jsp?sItemId=000001966831
Affiliation
대학원
Department
대학원 재료공학과
Advisor
문창권
Table Of Contents
Abstract

1. 서 론
1.1연구배경 및 목적
2. 이론적 배경
2.1 그라핀
2.2 그라핀의 합성
2.2.1 박리 그라핀 제조 기술
2.2.2 화학적 박리법 (modified Hummer's method)
2.3 XRD
2.4 EA
3. 실험방법
3.1 재료
3.2 Graphene 제조 방법
3.3 실험 조건
3.4 Graphene 특징 분석
- XRD, SEM, EA, 입도분석
4. 결과 및 고찰
4.1 산화 흑연 (graphite oxide)의 분석
4.2 그라핀의 반응 온도, 반응 시간, 초기 입자 크기에 따른 영향
5. 결 론

[참고문헌]
Degree
Master
Appears in Collections:
대학원 > 재료공학과
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