study on the fabrication of graphene using the exfoliation method
- Abstract
- The effect of various synthesis conditions in the fabrication of graphene using the exfoliation method has been investigated. The graphite oxide and graphene fabricated by various synthesis conditions were identified by SEM, FE-SEM and XRD. Graphite oxide was fabricated from graphite using chemical exfoliation and graphene was manufactured from graphite oxide by thermal exfoliation. As a result, graphite oxide was well formed from graphite and graphene could be obtained from graphite oxide. And it was found that the interlayer spacing between the graphene layers depended on the reaction time and particle size, regardless of the reaction temperature from 5℃ to 25℃.
- Author(s)
- 이정수
- Issued Date
- 2014
- Awarded Date
- 2014. 2
- Type
- Dissertation
- Publisher
- 부경대학교
- URI
- https://repository.pknu.ac.kr:8443/handle/2021.oak/1422
http://pknu.dcollection.net/jsp/common/DcLoOrgPer.jsp?sItemId=000001966831
- Affiliation
- 대학원
- Department
- 대학원 재료공학과
- Advisor
- 문창권
- Table Of Contents
- Abstract
1. 서 론
1.1연구배경 및 목적
2. 이론적 배경
2.1 그라핀
2.2 그라핀의 합성
2.2.1 박리 그라핀 제조 기술
2.2.2 화학적 박리법 (modified Hummer's method)
2.3 XRD
2.4 EA
3. 실험방법
3.1 재료
3.2 Graphene 제조 방법
3.3 실험 조건
3.4 Graphene 특징 분석
- XRD, SEM, EA, 입도분석
4. 결과 및 고찰
4.1 산화 흑연 (graphite oxide)의 분석
4.2 그라핀의 반응 온도, 반응 시간, 초기 입자 크기에 따른 영향
5. 결 론
[참고문헌]
- Degree
- Master
-
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- 대학원 > 재료공학과
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