Ni 분말이 함침된 TPU 및 열 경화형 에폭시 접착제의 유도가열 발열 거동 및 접착 특성에 관한 연구
- Alternative Title
- A study on Heating Behavior and Adhesion Property of Ni particle-embedded TPU and Thermosetting Epoxy Adhesive through Induction Heating
- Abstract
- Nowadays, in order to improve an efficiency of manufacturing process according to developing of technologies and industry, diverse studies have been vigorously conducting. Among a lot of industries, bonding process included in shoes, automobile or aircraft area is generally using convection oven method for heating the material. This method can be applied to consecutive processing for a large quantity of material as well as huge object such as automobile. However, because heat moves from surrounding air to adhesive through the object, object can be damaged thermally. Therefore, for replacing this heating method, a new method is needed for speedy and efficiency heating.
Induction heating is a method which heats the object using by high frequency alternating magnetic field (AMF). Because it is adopting the amf, it can be possible non-contact, selective and localized heating. Hence, induction heating was utilized in welding, annealing or melting of metal in the past, now it is being used for hyperthermia, electric stove as well as bonding between metal and polymer. When the induction heating is applied to shoe, automobile and aircraft industries, more efficient heating process can be possible by reducing the processing time.
In order to apply an induction heating method to manufacturing process, object should has a conductive or magnetic property. However, normal adhesive do not have these properties, so magnetic materials such as metal or ceramic should be embedded into the adhesive for generating heat. There are lots of studies about induction heating behavior of metal particles such as Fe, Ni, Co, Cu, Fe3O4. As a result, It was possible that controling the heat generation by regulating size, contents of particle, output of induction heater and adhesive thickness. Also, this heating method showed a faster heating speed and higer efficiency than oven heating.
In this paper, spherical type Ni particle with 70㎚, 1㎛, 70㎛ in size, flake and irregular type Ni particle with 1㎛ in size were used as a susceptor for observing an induction heating behavior and adhesion properties of TPU (Thermoplastic poly urethane) adhesive with respect to size, contents and shape of Ni. Furthermore, induction heating behavior and adhesion property of multi layered TPU adhesive with core layer in regard to content of Ni particle have been studied.
Additionally, induction heating behavior and adhesion property of one component epoxy adhesive with 70㎚ Ni spherical type particle also have been studied on thickness of adherend, content of Ni.
- Author(s)
- 임태규
- Issued Date
- 2020
- Awarded Date
- 2020. 2
- Type
- Dissertation
- Publisher
- 부경대학교
- URI
- https://repository.pknu.ac.kr:8443/handle/2021.oak/23737
http://pknu.dcollection.net/common/orgView/200000286550
- Alternative Author(s)
- TaeGyuIm
- Affiliation
- 부경대학교 대학원
- Department
- 대학원 화학융합공학부
- Advisor
- 손민영
- Table Of Contents
- Ⅰ. 서 론 1
Ⅱ. 이론 및 문헌 조사 3
2.1. 유도가열 발열 메커니즘 3
2.2. Curie Temperature 7
2.3. Skin effect 8
2.4. Failure mode 9
Ⅲ. 실 험 10
3.1. 원료 물질 10
3.2. 유도가열 용 접착제 제조 11
3.2.1. TPU 용액 및 접착제 필름 제조 11
3.2.2. 일액형 에폭시 접착제 제조 14
3.3. 유도가열 거동 및 접착 특성 분석 15
3.3.1. TPU 필름의 유도가열 승온 거동 및 접착 특성 분석 15
3.3.2. 에폭시 접착제의 유도가열 승온 거동 및 접착 특성 분석 16
Ⅳ. 결과 및 고찰 17
4.1. Ni 분말 크기 및 형상 분석 17
4.2. TPU 필름의 유도가열 승온 거동에 대한 Ni 분말의 영향 17
4.2.1. Ni 분말의 형상에 대한 영향 17
4.2.2. Ni 분말의 크기 변화에 대한 영향 23
4.2.3. Ni 분말의 함량 및 접착제 두께에 대한 영향 25
4.3. TPU 필름의 유도가열 접착 특성 분석 27
4.3.1. Ni 분말의 형상 변화에 따른 영향 27
4.3.2. Ni 분말의 크기 변화에 따른 영향 28
4.3.3. Ni 분말의 함량 및 접착제 두께 변화에 따른 영향 29
4.4. 다중 층 TPU 필름의 발열 층 밀도 변화에 따른 유도가열 거동 34
4.5. 다중 층 TPU 필름의 발열 층 밀도에 따른 접착 강도 분석 35
4.6. Ni 분말이 첨가된 일액형 에폭시 접착제의 유도가열 거동 분석 40
4.6.1. Ni 분말의 함량 변화에 따른 일액형 접착제의 유도가열 특성 40
4.6.2. 피착제의 두께 변화에 따른 유도가열 특성 40
4.7. Ni 분말이 첨가된 에폭시 접착제의 가열 방법에 따른 접착 특성 45
Ⅴ. 결론 49
참고문헌 51
- Degree
- Master
-
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