냉간가공에 따른 Fe-20Mn-12Cr-3Ni-3Si 합금의 기계적 특성 및 조직학적 특성에 미치는 영향
- Abstract
- There are two types of damping materials which are organic or metallic material. Shortage of organic materials that they are easily polluted by environment and their applications are limited by temperature and wavelength. Thus, metallic materials that have lower dependence on temperature and wavelength have highly been attentioned. Also, the metallic materials are classified with the type of composite, ferromagnetism, dislocation or etc. However, they still had the problem that low strength, complication of manufacturing process. From these reason, their application on industrial field have been inhibited. Moreover, in the most case, damping materials are need to endure the noise and vibration and have the high damping capacity and strength in sametime. Almost every metallic damping materials are hard to be satisfied that condition. Thus, the new materials that have high damping capacity, high strength, mechanical properties and corrosion resistance in sametime. Thus, as the fundamental research for the development of high strength and damping capacity material, the newly composed alloy were used in this study. Fe-20Mn-12Cr alloy was used and 3Ni and 3Si was adopted as an alloying element. Alloying elements were choosed for increasing corrosion resistance and stacking fault energy. Alloy were melted in vacumm furnace and manufactured to ingot. And then, they were hot rolled at 1200 to process for appropriate size of plate shape. Every plates was leansed in acid after annealing at 1050 1H and quenched for solid solution. Finally, they were cold rolled with different rolling reduciton but plate shape to 2mm thickness on the room temperature. They were used to investigate the relationship between microstructure and mechanical properties or damping capacity. The damping capacity was measured by electric discharge machining from a cold-rolled sample to a test piece having a size of 2 mm × 120 mm × 10 mm, and then, using a horizontal internal friction measurement device to obtain the logarithmic damping rate under vacuum. The microstructure of each specimens was obeserved using optical microscopy and scanning electron microscopy. Also, transmission electron microscopy was used for phase identification. After cold rolling,
After performing the cold working, martensite was generated by working from the previously formed austenite phase, which showed a larger amount as the working amount increased. In addition, martensite had two different phases, α′ and ε, and it was confirmed that they intersect or have directionality for a specific orientation. Of the two phases, α′ was initially formed, and as the stacking fault energy increased as processing proceeded, the fraction of the ε phase became higher. In this alloy, the damping properties were highly influenced by the ε phase. In particular, as the fraction of the ε phase increased, the interaction between austenite and the interface occurring in the ε phase, such as interfacial migration and the increase of stacking fault energy, increased, and the damping capacity characteristics increased. Changes in tensile properties such as strength in this alloy were also affected by the fraction of the ε phase, and as the fraction of the corresponding phase increased, its strength and elongation increased further.
- Author(s)
- 정종민
- Issued Date
- 2022
- Awarded Date
- 2022. 2
- Type
- Dissertation
- Publisher
- 부경대학교
- URI
- https://repository.pknu.ac.kr:8443/handle/2021.oak/24233
http://pknu.dcollection.net/common/orgView/200000606970
- Affiliation
- 부경대학교 대학원
- Department
- 대학원 금속공학과
- Advisor
- 김권후
- Table Of Contents
- 제 Ⅰ 장 서론 1
1.1. 연구배경 02
1.2. 연구목적 05
1.3. 연구내용 08
제 Ⅱ 장 이론적 배경 9
2.1. 마르텐사이트 변태 10
2.1.1. 마르텐사이트 변태의 구동력 12
2.1.2. 응력 유기 마르텐사이트 변태 16
2.1.3. 정벽면(habit plane) 18
2.2. 오스테나이트(FCC)→ε마르텐사이트(HCP) 변태 21
2.2.1. γ → ε 변태의 전단변형 특성 21
2.2.2. ε 마르텐사이트의 생성기구 22
2.2.3. ε 마르텐사이트의 자기조정(self-accommodation) 25
2.3. ε 마르텐사이트→ α' 마르텐사이트 변태 26
2.3.1. ε 마르텐사이트(HCP)→α'마르텐사이트(BCC) 변태 26
2.3.2. α' 마르텐사이트(BCC)의 성장 과정 28
2.4. 진동감쇠기구(Damping mechanism) 30
2.4.1. 동적 이력 기구(dynamic hysteresis mechanism) 32
2.4.2. 정적 이력 기구(static hysteresis mechanism) 35
2.4.3. 진동감쇠능을 표현하는 방법 35
2.5. 열탄성 마르텐사이트와 비열탄성 마르텐사이트 41
2.5.1. 열탄성 마르텐사이트 41
2.5.2. 비열탄성 마르텐사이트 46
제 Ⅲ 장 가공유기 마르텐사이트가 감쇠능에 미치는 영향 47
3.1. 서론 48
3.2. 실험방법 50
3.2.1. 시료(Specimens) 50
3.2.2. 미세조직의 관찰 50
3.2.3. 미세조직의 정량 분석 51
3.2.4. 감쇠능 측정 51
3.3. 실험결과 및 고찰 52
3.3.1. 미세조직 관찰 52
3.3.2. 미세조직과 감쇠능에 미치는 냉간 가공의 영향 58
3.3.3. 감쇠능에 미치는 마르텐사이트의 영향 61
3.4. 결론 66
제 Ⅳ 장 냉간가공이 인장특성에 미치는 영향 67
4.1. 서론 68
4.2. 실험 방법 70
4.2.1. 시료 및 열처리 70
4.2.2. 미세조직의 관찰 70
4.2.3. 미세조직의 정량 분석 71
4.2.4. 인장성질 측정 71
4.3. 실험 결과 및 고찰 72
4.3.1. 미세조직관찰 72
4.3.2. 미세조직과 인장성질에 미치는 냉간가공의 영향 78
4.3.3. 인장성질과 마르텐사이트의 상호관계 81
4.4. 결론 86
제 Ⅴ 장 결론 87
5. 결론 88
참고문헌 90
감사의 글 96
- Degree
- Doctor
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