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Plakett-Burman과 혼합물 실험계획법을 활용한 천연 육수 조미료 제조의 최적화

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Abstract
The convenience food market is growing due to social changes such as single-person households, women-entering society, and increasing nuclear families. In order to develop a natural seasoning product according to the social flow, the optimization of the mixing ratio was studied. Through statistical methods, it was possible to reduce the time and cost part by proceeding with minimal experiments. Using Plackett-Burman design among statistical methods, it was confirmed that shrimp, mushrooms and green onions are the main factors influencing taste and preference. When shrimp content was small and mushroom and green onion amounts were high, overall preference was high. Shrimp, mushrooms and green onions were designated as independent variables, and the optimum ratio of independent variables was confirmed through the mixture experiment planning. The best recipe was 0.25g anchovy, 0.15g dipori, 0.1g kelp, 0.09g shrimp, 0.15g mushroom, 0.05g garlic, 0.05g onion, 0.05g salt, 0.05g white radish and 0.06g green onion. The volatile fragrance components of the seasoning with the optimal blending ratio were detected with 9 aldehydes, 3 alcohols, 12 alkanes, and 6 others. The main fragrance components were propanal, 3-methylbutanal, allyl alcohol, and trimethylamine. 21 free amino acids were detected, and glutamic acid, the representative umami component, was the highest with 437.05 mg/100g, followed by taurine, arginine, aspartic acid, glutamin, alanine, histidine, and so on. This study can be used as a basis for developing a seasoning product that minimize time and cost consumption with a small number of experiments using statistical methods.
Author(s)
구나은
Issued Date
2020
Awarded Date
2020. 8
Type
Dissertation
Keyword
천연조미료 Plackett-Burman 혼합물 실험계획법
Publisher
부경대학교
URI
https://repository.pknu.ac.kr:8443/handle/2021.oak/2490
http://pknu.dcollection.net/common/orgView/200000339443
Alternative Author(s)
Na Eun Gu
Affiliation
부경대학교 글로벌수산대학원
Department
글로벌수산대학원 식품산업공학과
Advisor
이양봉
Table Of Contents
제 1장. Plackett-Burman Design을 이용한 천연 육수 조미료 레시피의 최적화 1
Ⅰ. 서론 1
Ⅱ. 재료 및 방법 6
1. 실험재료 6
2. 실험방법 6
2.1. Plackett-Burman Design을 이용한 천연 육수 조미료 제조 6
2.2. 관능평가 9
2.3. 통계처리 11
Ⅲ. 결과 및 고찰 12
1. 천연 육수 조미료의 관능평가에 의한 구성성분에 대한 영향 12
2. Plackett-Burman Design을 이용한 천연 육수 조미료 관능평가 결과 15
Ⅳ. 결론 18
제 2장. 혼합물 계획법을 이용한 천연 육수 조미료 제조의 최적화 19
Ⅰ. 재료 및 방법 19
1. 실험재료 19
2. 실험방법 20
2.1. 혼합물 계획법을 이용한 천연 육수 조미료 제조 20
2.2. 관능평가 24
2.3. 통계처리 25
2.4. 일반성분 25
2.5. 색도 측정 26
2.6. pH 측정 26
2.7. 식염 함량 26
2.8. GC-MS를 이용한 천연 육수 조미료의 휘발성 향기성분 분석 27
2.9. 천연 육수 조미료 유리아미노산 분석 29
Ⅱ. 결과 및 고찰 31
1. 혼합물 계획법을 이용한 천연 육수 조미료 분석 결과 31
2. 혼합물 계획법을 이용한 천연 육수 조미료 관능평가 결과 34
3. 일반성분 결과 41
4. pH 및 색도, 식염 결과 41
5. 최적화된 천연 육수 조미료의 휘발성 향기성분 측정 결과 43
6. 최적화된 천연 육수 조미료의 유리아미노산 분석 결과 48
Ⅲ. 결론 51
Ⅳ. 참고문헌 54
Degree
Master
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글로벌수산대학원 > 식품산업공학과
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