PUKYONG

DIC기법의 미소균열 적용 및 분석 방법 개발에 관한 연구

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Alternative Title
A study on the development of analysis methods and application of DIC technique to micro cracks
Abstract
Defects in devices, structures, and materials affect their performance and safety. In order to identify and evaluate these defects, strain measurement is necessary. The strain measurements of cracks estimate the material properties and occurrence of cracks in the structure. The purpose of this study is to apply the DIC method to various materials to increase the measurement accuracy for deformation and find crack initiation. A 3-point bending test was performed on brass specimens with different speckle concentrations to study the effects of speckle patterns on DIC evaluation. Through GLCM evaluation, it was confirmed that the contrast showed the maximum value at about 35∼50%, and the maximum value of entropy remained constant after about 35%. The elastic modulus and tensile strength were very similar between measurements using an electrical resistive strain gauge and DIC analysis at 35% contrast. Furthermore, 3-point bending experiments were conducted using composite materials that combine carbon fiber and aluminum liner. The strain was evaluated by the DIC method, and the occurrence of micro cracks in the specimens was measured. In the case of specimens with an inserted notch crack, cracks occurred at the notch crack tip, and delamination proceeded along the CFRP laminate interface. The initial micro cracks in specimens with different stacking orders measured 58.8 ㎛ and 53 ㎛, respectively, indicating crack growth in non continuous jump cases of strain rate. Moreover, DIC analysis was also performed on SOFC material with Ag paste as a current collector under high temperature conditions. As the experimental temperature increased, the crack initiation load and displacement also increased. Cracks occurred at the notch, and delamination between the Ag paste and the SiO₂wafer was observed. Additionally, the Ag paste exhibited ductility at low temperatures, but hardened and increased in stiffness as the temperature rose. Cracks began to advance toward the Ag paste at the initial notch crack tip, and interfacial separation progressed in the transverse direction along the laminated surface in the Ag paste. The micro crack length information was obtained by applying ACDM and Image J after conducting DIC analysis on SOFC.
Author(s)
이준혁
Issued Date
2023
Awarded Date
2023-08
Type
Dissertation
Publisher
부경대학교
URI
https://repository.pknu.ac.kr:8443/handle/2021.oak/33253
http://pknu.dcollection.net/common/orgView/200000694904
Affiliation
부경대학교 대학원
Department
대학원 안전공학과
Advisor
권오헌
Table Of Contents
1. 서 론 1
1.1 연구 배경 1
1.2 구조물 변형과 파손 해석 3
1.2.1 파괴역학 3
1.2.2 복합재료 7
1.3 파괴 평가 수법 13
1.3.1 평가 수법 13
1.3.2 스펙클 패턴(speckle pattern) 15
1.4 연구의 목적 18
2. 배경 이론 20
2.1 DIC 20
2.1.1 DIC 특징 20
2.1.2 DIC 이론 및 평가방법 21
2.2 균열 측정 평가수법 30
2.2.1 GLCM 30
2.2.2 ACDM 31
3. 실험 설계 및 방법 38
3.1 시험편 38
3.1.1 스펙클 패턴 형성 및 황동 실험편 38
3.1.2 CFRP 하이브리드 복합재 42
3.1.3 고체연료전지 47
3.2 실험 방법 50
3.2.1 인장실험 50
3.2.2 3점 굽힘실험 53
3.2.3 4점 굽힘실험 55
4. 결과 및 고찰 63
4.1 DIC 스펙클 형상에 따른 영향 평가 63
4.1.1 스펙클 패턴 농도에 따른 GLCM평가 63
4.1.2 인장실험 결과 66
4.1.3 미소균열측정 평가 70
4.1.4 소결 75
4.2 탄소섬유 복합재료 균열 측정 76
4.2.1 노치가 없는 시험편의 균열 발생 76
4.2.2 초기 균열 시험편의 균열진전 평가 79
4.2.3 시험편 적층 방향의 영향 83
4.2.4 소결 88
4.3 고온환경에서 연료전지 계면 균열 측정 평가 89
4.3.1 실험온도에 따른 하중 및 균열 발생 평가 89
4.3.2 고온상태의 고체산화물 연료전지 전극측 계면에서의 DIC평가 93
4.3.3 Ag 페이스트에 대한 SEM 분석결과 98
4.3.4 ACDM 균열진전평가 100
4.3.5 소결 103
5. 결 론 104
Degree
Doctor
Appears in Collections:
대학원 > 안전공학과
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