Y2O3를 혼합한 치과용 합금의 미세조직 및 기계적 특성
- Abstract
- The mechanical properties and corrosion resistance of existing casting alloys are reduced due to defects such as bubbles and coagulation shrinkage during casting, and to compensate for these shortcomings, various attempts have been made to improve mechanical properties, corrosion resistance, and machinability by utilizing powder metallurgy alloying processes. The processing method of dental alloys is changing from analogue methods such as investing, burn-out, casting, devesting to digital methods such as metal milling and 3D printers. Therefore, recognizing the importance of developing dental alloys, specimens based on the composition ratio of three types of dental alloys (implant abutment, PFM, and denture frame) were fabricated by powder metallurgy process to conduct a comparative evaluation of material properties. The mechanical alloying process is a useful method for developing new alloys because it is easier to control microstructure by controlling added elements than casting. The effects of powder metallurgy and reinforcement additions on the mechanical properties of dental metallic materials were reviewed. Based on the dental commercial alloys Ti-6Al-4V, Co-25Cr, and Ni-26Cr alloy chemical compositions, mechanical alloying process was performed by mixing each component powder with Y2O3 powder. The powder was prepared into alloy specimens by uniaxial pressure molding at a 1100 ℃ for 2 hours. The prepared specimens were cut to observe the microstructure, and hardness measurements and tensile tests were performed to compare with commercial materials.
- Author(s)
- 홍혜란
- Issued Date
- 2024
- Awarded Date
- 2024-02
- Type
- Dissertation
- Keyword
- Dental alloy, oxide dispersion strengthening, mechanical alloying, hardness, tensile strength
- Publisher
- 국립부경대학교 산업대학원
- URI
- https://repository.pknu.ac.kr:8443/handle/2021.oak/33639
http://pknu.dcollection.net/common/orgView/200000742677
- Affiliation
- 국립부경대학교 산업대학원
- Department
- 산업대학원 재료공학과
- Advisor
- 노상훈
- Table Of Contents
- Ⅰ. 서 론 1
Ⅱ. 이론적 배경 3
1. 치과용 재료의 가공 시스템 및 합금조건 3
2. 산화물 분산 강화 합금 19
3. 강의 강화 기구 21
3.1 결정립계에 의한 강화 21
3.2 고용에 의한 강화 25
3.3 미세한 입자에 의한 강화 28
Ⅲ. 실험방법 31
1. 합금 제작 31
2. 미세조직 관찰 및 특성평가 35
2.1 미세조직 분석 35
2.2 인장 특성 평가 35
2.3 경도 측정 40
2.4 밀도 측정 44
3. 밀링 시험 44
Ⅳ. 실험 결과 및 고찰 47
1. Ti 합금 47
1.1 분말 형상 관찰 47
1.2 Ti 합금 미세조직 51
1.3 Ti 합금 기계적 특성 58
2. Ni-Cr 합금 62
2.1 분말 형상 관찰 62
2.2 Ni-Cr 합금 미세조직 64
2.3 Ni-Cr 합금 기계적 특성 73
3. Co-Cr 합금 77
3.1 분말 형상 관찰 77
3.2 Co-Cr 합금 미세조직 79
3.3 Co-Cr 합금 기계적 특성 88
4. 밀링시험 결과 92
Ⅴ. 결 론 93
Ⅵ. 참고문헌 95
감사의 글 98
- Degree
- Master
-
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